NMR Facilities

Bruker Ascend™ 700 MHz spectrometer

The Chemistry Department at Stony Brook University houses in the basement of the chemistry building a recently purchased Bruker Ascend™ 700 MHz spectrometer, equipped with a variable temperature accessory, a digital temperature control unit and Z-gradient electronics. Two probes are available for this instrument

Inverse Triple Resonance (TXI)

A room temperature Inverse Triple Resonance (TXI) 5 mm Probe for 1H observation and 13C and 15N decoupling, equipped with automatic tuning and matching module, and Z-gradient.

Quadruple Resonance (QCI)

A Quadruple Resonance (QCI) 13C-enhanced 5 mm CryoProbe for 1H observation with 13C, 15N and 31P decoupling, equipped with automatic tuning and matching module, and Z-gradient.

Bruker Ascend™ 700 MHz spectrometer

Bruker Ascend™ 700 MHz spectrometer

Bruker 500 MHz spectrometer

Bruker 500 MHz spectrometer

Bruker 500 MHz spectrometer

A 500 MHz spectrometer recently upgraded with a Bruker Avance III Console equipped with a variable temperature accessory, a digital temperature control unit and Z-gradient electronics. Probes available for this instrument are

Inverse Triple Resonance Broadband (TBI)

A room temperature Inverse Triple Resonance Broadband (TBI) 5 mm Probe for 1H observation and 13C and BB decoupling (tunable from 15N to 31P) equipped with Z-gradient.

SmartProbe™

A room temperature SmartProbe™ (5 mm) for X-nucleus observation tunable from 15N to 31P as well as 19F with 1H decoupling and observation, equipped with automatic tuning and matching module and Z-gradient.

CryoProbe Prodigy™

A CryoProbe Prodigy™ (5 mm) for X-nucleus observation tunable from 15N to 31P with 1H or 19F decoupling and observation, equipped with and automatic tuning and matching and Z-gradient.

Bruker 400 MHz spectrometer

A 400 MHz spectrometer recently upgraded with a Bruker Nanobay Console equipped with a variable temperature accessory, a digital temperature control unit and Z-gradient electronics. This instrument has a BBFOPLUS 5 mm probe optimal for X-nucleus observation tunable from 15N to 31P as well as 19F with 1H decoupling and observation, equipped with Z-gradient and automatic tuning and matching

Bruker 400 MHz spectrometer

Bruker 400 MHz spectrometer

Bruker 300 MHz Ultra-Shield Fourier spectrometer

Bruker 300 MHz Ultra-Shield Fourier spectrometer

Bruker 300 MHz Ultra-Shield Fourier spectrometer

A new Bruker 300 MHz Ultra-Shield Fourier spectrometer equipped with 1H and 13C amplifiers, variable temperature Control and Z-gradient electronics. A Room Temperature Fourier Dual 5 mm Probe for 13C-nucleus observation with 1H decoupling and observation and Z-gradient is currently installed on this instrument.

Varian Gemini 300 MHz spectrometer

Additionally, an older 300 MHz spectrometer operating with a Varian Gemini 2300 gradient console operating with a probe configured for observation of 1H, 13C, 19F, and 31P nuclei, completes the list of NMR spectrometers at the Chemistry Department.

Mass Spectrometer

Our synthetic programs are facilitated by state-of-the-art mass spectrometry instrumentation. We are fortunate to have both instrumentation and expertise available within the Chemistry building at Stony Brook University

The departmental mass spectrometry instrumentation

  • Bruker AutoFlex II MALDI-TOF/TOF.
  • Agilent 5973 MSD/6890 Series GC.
  • Agilent 1100 LC/MSD.

The proteomics facility

  • Thermo Fisher Scientific LTQ Orbitrap XL ETD
  • Applied Biosystem Voyager DE-STR MALDI-TOF
  • Thermo Fisher Scientific LTQ XL
  • Thermo Fisher Scientific TSQ Quantum Access triple quadrupole

Waters High Performance Liquid Chromatography

Fourier Transform Infrared Spectrometer

Diode Array Ultraviolet spectrometers

Center for DNA synthesis